Curriculum | Pharmaceutical Analysis I Practical | B. Pharmacy

  B. Pharmacy Semester- 1st /1st Year  
  Subject: Pharmaceutical Analysis -I–Practical  
  Subject Code: BP108 P  
S. No Contents of the Topics Learning Objectives Teaching Guidelines Methodology Assessment Tools Time Allocated
1 Preparation and standardization of

Sodium hydroxide

Sulphuric acid

Sodium thiosulfate

Potassium permanganate

Ceric ammonium sulphate

(At the end of the practical  the student should be able to)

 

Prepare and standardize various compounds ,know their properties, assay procedure  &  applications

Preparation and standardization of

Sodium hydroxide

Sulphuric acid

Sodium thiosulfate

Potassium permanganate

Ceric ammonium sulphate

Instructive, Demo in lab Experiment performance,

Viva voce & result

15
2 Assay of the following compounds along with Standardization of Titrant

Ammonium chloride by acid base titration

Ferrous sulphate by Cerimetry

Copper sulphate by Iodometry

Calcium gluconate by complexometry

Hydrogen peroxide by Permanganometry

Sodium benzoate by non-aqueous titration

Sodium Chloride by precipitation titration

Explain Assay of various inorganic compounds along with standardization of titrant (preparation methods, test ,properties& uses) Assay of the compounds along with Standardization of Titrant

 

Instructive, Demo in lab Experiment performance,

Viva voce & result

21
3 Determination of Normality by electro-analytical methods

Conductometric titration of strong acid against strong base

Conductometric titration of strong acid and weak acid against strong base

Potentiometric titration of strong acid against strong base

 

 

 

 

Working on conductometer & Potentiometer and determine the normality for strong acid against strong base , strong acid and weak acid against strong base, strong acid against strong base

 

 

Determination of Normality by electro-analytical methods

 

Instructive, Demo in lab Experiment performance,

Viva voce & result

09
Admission 2017